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Determination of Prulifloxacin by Miniaturized Nonaqueous Titration |
Liu Xiuqing, Ren Chunxiao |
Heilongjiang Provincial Drug Audit and Inspection Center,Harbin 150090,China |
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Abstract Objective To explore the determination of prulifloxacin by miniaturized non-aqueous titration.Methods The miniaturized non-aqueous titration method and the major non-aqueous titration method were used to determine the content of rulifloxacin,and the accuracy and precision of the two Methodswere compared.Results Constant and miniaturized Methodswere used to repeat the measurement for 6 times,respectively.The mean value of the data measured by the constant method was 95.8%,and the relative standard deviation was 0.8%.The stability test showed that there was no significant difference between each data within 0-5h(P>0.05).Conclusion Using miniaturized non-water drop to determine drug content can stabilize energy consumption and control method is practical.
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Received: 15 June 2021
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[1] 张才煜,宁保明,何兰.核磁共振定量法在化学对照品标化中的应用[J].药物分析杂志,2019,39(5):165-170. [2] 潘东,邢士超,徐杰丰,等.简易滴定法治疗阿片类药物耐受癌痛的疗效分析[J].浙江医学,2019,41(14):1541-1544. [3] 马奋刚,张永萍,曹国琼,等.HPLC法测定化风丹药母在发酵过程中6个酯型生物碱的含量[J].药物分析杂志,2020,40(3):413-419. [4] 马开,田萍,张迪文,等.波长切换HPLC法同时测定六神曲中9个成分的含量[J].药物分析杂志,2019,39(3):526-530. [5] 王彦娥,高娟.微型化非水滴定法在药品含量测定中的应用[J].世界最新医学信息文摘,2017,21(46):125. |
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